Separation of Aliphatic Alcohols by Paired Ion Liquid Chromatography.

Abstract

Using the cationic dye, methylene blue (as the chloride salt) to enhance the sensitivity of detection of species not possessing chromophores as a .0001 M component of a methanol/water mobile phase, a series of alcohols from ethanol to t-pentanol were separated on Partisil ODS with good baseline separation at submicrogram levels using spectrophotometric detection at 651 nm. A retention model based on dye-alcohol complex formation and equilibrium partitioning of these species is advanced.

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Document Details

Document Type
Technical Report
Publication Date
Jan 01, 1981
Accession Number
ADA116806

Entities

People

  • H. Freiser
  • T. Gnanasambandan

Organizations

  • University of Arizona

Tags

DTIC Thesaurus Topics

  • Alcohols
  • Analytical Chemistry
  • Chemical Synthesis
  • Chemistry
  • Chromatographs
  • Chromatography
  • Detection
  • Detectors
  • Dyes
  • Equations
  • Flow Rate
  • Liquid Chromatography
  • Materials
  • Materials Science
  • Methanols
  • Organic Chemistry
  • Solvent Extraction

Fields of Study

  • Chemistry

Readers

  • Analytical Chemistry