Micrographic Observations of the Carbonaceous Mesophase by a Quenching Hot Stage.
Abstract
A hot-stage microscope with quenching capability was employed to relate the observations made at the free surface of a pitch during pyrolysis to the bulk microstructure. Freshly formed mesophase spherules display an 'iceberg effect' with only a limited upper segment exposed to view. The mesophase layers tend to lie normal to the free surface, and + or - 2 Pi as well as + or - Pi disclinations display discontinuous cores at the free surface; aside from these minor effects, surface observations appear to be representative of events taking place within the bulk mesophase. (Author)
Document Details
- Document Type
- Technical Report
- Publication Date
- Aug 30, 1982
- Accession Number
- ADA119793
Entities
People
- Cassandra B. Ng
- Jack L. White
- Manfred Buechler
Organizations
- The Aerospace Corporation