Surface Sampling Techniques

Abstract

This study resulted in the development of several methods for the sampling and analysis of explosives/explosive residues on building materials surfaces. A method for qualitative determination based on detection of charge- transfer complexes formed between the explosive/explosive residue and a visualization reagent applied to the surface has been evaluated in the field at two Army Ammunition Plants. A method for quantitative determination based on solvent extraction of samples collected in the field followed by high pressure liquid chromatographic analysis has been evaluated on samples prepared in the laboratory, and found to give promising results. The theoretical and practical feasibility of another method for qualitative determination based on UV irradiation of a suspected contaminated surface with subsequent detection of any explosives/explosive residues present has been demonstrated. This approach may provide the means for 'scanning' an area to determine whether explosives are present on a real-time basis. Further development of this approach is recommended.

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Document Details

Document Type
Technical Report
Publication Date
Sep 01, 1982
Accession Number
ADA120857

Entities

People

  • Bruce E. Goodwin
  • Emmett M. Smith
  • James R. Aronson
  • Margaret A. Randel
  • Robert P. O'neil

Organizations

  • Arthur D. Little

Tags

Communities of Interest

  • Biomedical
  • Counter IED
  • Weapons Technologies

DTIC Thesaurus Topics

  • Aromatic Hydrocarbons
  • Chemical Analysis
  • Chemical Reactions
  • Chemical Synthesis
  • Chemistry
  • Chromatographs
  • Crystal Structure
  • Detectors
  • Explosives
  • Materials Laboratories
  • Materials Science
  • Materials Testing
  • Measurement
  • Plastic Explosives
  • Rodents
  • Solvent Extraction
  • Test Methods

Readers

  • Agricultural Chemistry/Soil Science
  • Electrochemical Engineering/ Fuel Cell Technologies
  • Systems Analysis and Design