Analytical Methods Development for Dimethyl Methylphosphonate, Diisopropyl Methylphosphonate and Trimethyl phosphate.

Abstract

A gas chromatographic system employing a Flame Photometric Detector (GC/FPD) was used to develop a method for the determination of Dimethyl methylphosphonate (DMMP), Diisorpropyl methylphosphonate (DIMP) and Trimethyl phosphate (TMP) in aqueous samples under Task R902.35.14. The precision and accuracy of the developed method was determined from the analysis of aqueous samples spiked with 4.92 to 98.40 micron g/L of DIMP in the presence of 10 mg/L each of DMMP and TMP. The detection limit at the 90% confidence level, calculated by the method of Hubaux and Vos, is 9.05 micron g/L of DIMP in the presence of 10 mg/L each of DMMP and TMP. (Author)

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Document Details

Document Type
Technical Report
Publication Date
Sep 01, 1982
Accession Number
ADA120863

Entities

People

  • Carol Wong
  • Linda Sadowski
  • Margaret Randel
  • Rose Fasano

Organizations

  • Arthur D. Little

Tags

DTIC Thesaurus Topics

  • Accuracy
  • Boiling Point
  • Calibration
  • Chemical Synthesis
  • Chemistry
  • Chlorides
  • Data Sets
  • Detection
  • Detectors
  • Logistics Management
  • Methylphosphonates
  • Precision
  • Rocky Mountains
  • Standards
  • Surface Waters
  • Technical Information Centers
  • Water

Fields of Study

  • Agricultural and Food sciences
  • Chemistry

Readers

  • Analytical Chemistry