Detection of T-2 Toxin by a Modified Radioimmunoassay.
Abstract
T-2 toxin in serum, urine and saline was analyzed by a modified radioimmuno-assay procedure. The specimens were added directly to the assay tubes without extraction steps. The reaction between antibody and ligands was optimized at one hour. Albumin-coated charcoal was used to separate bound from free radioactivity. Quenching which occurred with hemolyzed specimens was corrected with a wet oxidation process using 60% perchloric acid and 30% hydrogen peroxide. The shorter incubation times resulted in an assay that takes less than 6 h to complete. The average affinity constant of the antibody (km) was 1.75 x (10 to the 10th power) liters/mol. The sensitivity was 1 ng per assay or 10 ng/mi. Among the other trichothecenes tested only H T-2 cross-reacted significantly.
Document Details
- Document Type
- Technical Report
- Publication Date
- Aug 06, 1982
- Accession Number
- ADA123195
Entities
People
- David L. Bunner
- Fun Sun Chu
- Joanne Beheler
- Paulito A. Fontelo
Organizations
- United States Army Medical Research Institute of Infectious Diseases