Aerosol Direct Fluorination-Synthesis of Perfluoroadamantane the Penultimate Step.
Abstract
The aerosol direct fluorination technique has been successfully employed to convert adamantane to perfluoroadamantane in 28% overall yeilds based on input. Although physical losses in the reactor reduced yields the major (74.4%) product collected was perfluoroadamantane. Fragmentation and ring-opening proved to be insignificant as was the proportion of 1-hydrylpentadecafluoroadamantane. (Author)
Document Details
- Document Type
- Technical Report
- Publication Date
- Feb 25, 1983
- Accession Number
- ADA129364
Entities
People
- James L. Adcock
- Mark L. Robin
Organizations
- University of Tennessee system