Durable Copper Polyimide Adhesive Bonds

Abstract

With an optimum chemically converted surface on copper, durable structural adhesive bonds can be produced. By this particular alkaline oxidizing formulation and post-sealing, excellent structural bonds, which are both thermally and chemically stable, are achieved. The stability of these oxidized surfaces has been demonstrated through extensive tensile lap shear, interlaminar shear testing, and verifying peel tests. Although bonding has been primarily evaluated with a polyimide adhesive, the effect of the hot alkaline oxidizing solution on epoxy fiberglass substrates was explored using the ASTM interlaminar shear bending test and electrical resistance comb pattern. Quantitative analytical procedures for constituents in the alkaline oxidizing bath are described.

Open PDF

Document Details

Document Type
Technical Report
Publication Date
May 24, 1983
Accession Number
ADA130221

Entities

People

  • Allan E. Mason
  • Edward B. Murphy
  • Edward S. Wainwright

Organizations

  • Massachusetts Institute of Technology

Tags

Communities of Interest

  • Advanced Electronics

DTIC Thesaurus Topics

  • Adhesion
  • Adhesive Bonding
  • Adhesives
  • Air Force
  • Bonding
  • Chemical Analysis
  • Circuit Boards
  • Circuits
  • Coatings
  • Copper Oxides
  • Electron Microscopes
  • High Temperature
  • New Hampshire
  • Printed Circuits
  • Scanning Electron Microscopes
  • Shear Tests
  • United States

Fields of Study

  • Materials science

Readers

  • Organic Chemistry
  • Reinforced Composite Materials