Detection of T-2 Toxin by an Improved Radioimmunoassay

Abstract

T-2 toxin in serum, urine, and saline was analyzed by a modified radioimmunoassay procedure. The specimens were added directly to the assay tubes without extraction steps. The reaction between antibody and ligands was optimal at 1-h. Albumin-coated charcoal was used to separate bound from free radioactivity. Quenching, which occurred with hemolyzed specimens, was corrected by a wet oxidation process with 60% perchloric acid and 30% hydrogen peroxide. The shorter incubation times resulted in an assay that takes less than 6 h to complete. The average affinity constant of the antibody (K sub m) was 1.75 x 10 (expn 10) liters/mol. The sensitivity was 1 ng per assay or 10 ng/ml. Among the other trichothecenes tested, only H-T-2 cross-reacted significantly (10.3%).

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Document Details

Document Type
Technical Report
Publication Date
Feb 01, 1983
Accession Number
ADA133843

Entities

People

  • David L. Bunner
  • Fun Sun Chu
  • Joanne Beheler
  • Paulito A. Fontelo

Organizations

  • United States Army Medical Research Institute of Infectious Diseases

Tags

DTIC Thesaurus Topics

  • Albumins
  • Antibodies
  • Detection
  • Fungi
  • Health
  • Immune Serums
  • Medical Personnel
  • Oxidation
  • Perchloric Acid
  • Production
  • Public Health
  • Radioimmunoassay
  • Rocket Oxidizers
  • Saturation
  • Scintillation
  • Scintillation Counters
  • Standards

Fields of Study

  • Biology

Readers

  • Analytical Chemistry
  • Mathematics or Statistics
  • Molecular and Cellular Biochemistry