Binuclear Schiff Base Complexes of m-Xylylenebis(2-(1,3-Propanedi (2-Pyridinealdmine))) and M-Xylylenebis(2-(1,3-Propanedi(2-Pyrrolealdmine))).
Abstract
Binulcear complexes of Ni, Cu, and Co have been synthesized and characterized. The reaction of nickel(II)-, copper (II)-, or cobalt(II)chloride with a solution of 2-pyridinealdehyde and m-xylylenebis(2-(2,3-propanediamine) results in the formation of Ni2LC14(2a), Cu2LC14 (3) and Co2LC14(4), respectively, where L = m-xylylenebis(2-(2,3-propanedi(2-pyridinealdimine))). The binuclear nickel complexes, Ni2L(N3)4 (2b) and Ni2L(SCN)4 (2c) are prepared by metathesis of the chloride ion of complex 2a using the appropriate sodium salt. These complexes, 2-4, exhibit electronic spectra consistent with tetragonally distorted six-coordinate complexes.
Document Details
- Document Type
- Technical Report
- Publication Date
- Nov 04, 1983
- Accession Number
- ADA135507
Entities
People
- B. C. Whitmore
- R. Eisenberg
Organizations
- University of Rochester