Development of FT-IR Attenuated Total Internal Reflection Dichroism Techniques for Structural Characterization of Polymer Surfaces.
Abstract
We describe our continuing effort to develop FT-IR attenuated total reflection (ATR) dichroism techniques for the characterization of polymer surface structure and molecular orientation. Following theoretical background, we review the two-dimensional and three-dimensional analyses work based on a specially designed internal reflection crystal and a specially built ATR-sample attachment. In the current development section, we describe briefly the intensity correction procedures used in variable angle studies and an attempt to design a hemispheric crystal attachment to eliminate problems encountered with face-cut reflection crystals.
Document Details
- Document Type
- Technical Report
- Publication Date
- Apr 17, 1984
- Accession Number
- ADA140805
Entities
People
- C. S. P. Sung
- J. P. Hobbs
Organizations
- Massachusetts Institute of Technology