Strengthening and Strength Uniformity of Structural Ceramics

Abstract

The goal of this work is to identify the processing flaws that limit the strength of sintered ceramics, and to engineer uniform microstructures which either eliminate or minimize the size of these processing flaws. During the first year, a major advance was made by uncovering the fact that agglomerates in powders produce crack-like voids that severely limit the strength of sintered ceramics. Crack-like voids produced by the differential sintering of agglomerates relative to their surrounding powder matrix can be the most detrimental strength degrading flaw in sintered ceramics. As detailed and summarized in the review prepared for a 1984 ASM Conference on Materials for Future Energy Systems, colloidal approaches to powder processing and consolidation can minimize the size of soft agglomerates (those that can be broken apart with surfactants) and hard agglomerates (eliminated by sedimentation of colloidal suspensions). Work has shown that the elimination of the large, soft agglomerates with surfactants increases the average strength of a transformation toughened Al2O3/30 v/o ZrO2 (2.5 v/o Y2O3) composite from 550 MPa (80,000 psi) to 930 MPa (135,000 psi).

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Document Details

Document Type
Technical Report
Publication Date
Apr 01, 1984
Accession Number
ADA144302

Entities

People

  • F. F. Lange

Tags

Communities of Interest

  • C4I
  • Energy and Power Technologies
  • Weapons Technologies

DTIC Thesaurus Topics

  • Ceramic Materials
  • Chemical Reactions
  • Chemistry
  • Electron Microscopes
  • Fabrication
  • Heat Treatment
  • Material Degradation Processes
  • Materials
  • Materials Engineering
  • Materials Laboratories
  • Materials Processing
  • Materials Science
  • Mechanical Properties
  • Mechanical Working
  • Mechanics
  • Microscopes
  • Technical Ceramics

Fields of Study

  • Materials science

Readers

  • Nanocomposite Materials Science
  • Powder metallurgy of Titanium alloys.