An Investigation of a Cryogenic Matrix Isolation Approach for Characterizing Phosphorus Acid Aerosol.

Abstract

A matrix isolation cryostat has been adapted to sample gas streams containing aerosols for the latters subsequent analysis by infrared spectroscopy. The aerosol sampling was made in basically one of two modes: (1) the aerosol and its carrier gas were both condensed at 10K on the IR-transmitting surface, or (2) the aerosol alone was condensed on the IR-transmitting surface maintained at a temperature insufficient to condense the carrier gas. IR spectra of the condensed air + aerosol, or the aerosol alone, were then obtained. By suitably varying the temperature of the IR-transmitting surface, the air was distilled off leaving the aerosol behind. For aqueous aerosols containing non volatile solutes, the water could be partially or completely removed by raising the temperature of the condensed material to approximately 200K, followed by recooling to 10K for spectral analyses.

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Document Details

Document Type
Technical Report
Publication Date
Jul 01, 1984
Accession Number
ADA146188

Entities

People

  • A. Snelson

Organizations

  • IIT Research Institute

Tags

Communities of Interest

  • Air Platforms

DTIC Thesaurus Topics

  • Absorption
  • Aqueous Solutions
  • Electromagnetic Radiation
  • Frequency
  • Frequency Shift
  • Humidity
  • Hydrogen
  • Materials
  • Measurement
  • Particle Size
  • Particles
  • Phosphoric Acids
  • Phosphorus Acids
  • Spectra
  • Spectroscopy
  • United States
  • Water Vapor

Readers

  • Aerosol Science/Aerosol Physics
  • Analytical Chemistry
  • Thermal Physics or Thermal Science.