Mold and Crucible Coatings

Abstract

This report details the investigation of coating materials and their application to the graphite crucible and molds used in melting and casting DU-0. 75 Ti Alloy. Different types of washes were investigated: zirconium oxide, zirconium silicate, yttrium oxide, titanium carbide ( used as an undercoat), and boron nitride. The parameters investigated in the application of these coatings were number of burnouts of the crucible, method of cleaning, surface condition of the crucible, temperature of the crucible during painting, number and time between coats, and method of drying the crucible. The method of applying the wash affects its adherence to the graphite. The more thorough the drying of the first coat, the more effectively the coating protects the crucible. Drying in still air was detrimental to the success of most washes. Both oven or vacuum drying of the coated crucibles improved the adherence of most washes. Performance of yttrium oxide washes was dependent on the physical properties of the CMC binders. Yttria coating of the molds improved ingot surface quality, compared with zirconia coated or uncoated molds. Generally zirconium oxide washes outperformed titanium carbide under coated systems and yttrium oxide washes in the elevated temperature tests and in chemistry and ultrasonic results. Keywords: Depleted Uranium (DU); Ceramic Coatings; Graphite Coatings; MMT - Process improvement; Large caliber penetrators.

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Document Details

Document Type
Technical Report
Publication Date
Apr 28, 1986
Accession Number
ADA167864

Entities

People

  • Arthur L. Geary
  • Sylvia J. Canino

Tags

Communities of Interest

  • Advanced Electronics
  • Human Systems
  • Weapons Technologies

DTIC Thesaurus Topics

  • Adhesion
  • Ceramic Coatings
  • Ceramic Materials
  • Chemical Analysis
  • Chemical Synthesis
  • Chemistry
  • Economic Analysis
  • Materials
  • Materials Science
  • Particle Size
  • Physical Properties
  • Production Engineering
  • Standards
  • Surface Properties
  • Test And Evaluation
  • Yttrium Oxides
  • Zirconium Oxides

Fields of Study

  • Materials science

Readers

  • Materials Science and Engineering.
  • Surface Engineering/Surface Coating Technology.