The Effect of High Pressure on Electrical Relaxation in PPO and Electrical Conductivity in PPO Complexed with Lithium Salts.

Abstract

Audio frequency electrical conductivity and relaxation studies have been carried out on Parel 58 elastomer and Parel 58 elastomer complexed with a variety of lithium salts. The measurements have been carried out in vacuum over the temperature range 5-380 K and at pressures up to 0.65 GPA over the temperature range 230-380 K. Both the electrical conductivity for the complexed material and the electrical relaxation time associated with the alpha relaxation in the uncomplexed material exhibit VTF or WLF behavior. From the VTF analysis for both the vacuum electrical relaxation time and electrical conductivity, E sub a is found to be about 0.09 eV and T sub o is found to be about 40 C below the central glass transition temperature. In addition, it is found that the activation volumes for the electrical relaxation time and the electrical conductivity are the same when compared relative to t sub o. These results imply that the mechanism controlling ionic conductivity is the same as that for the alpha relaxation namely large scale segmental motions of the polymer chain. Keywords: Solid electrolytes, polymer electrolytes, poly(propylene oxide), activation energy.

Open PDF

Document Details

Document Type
Technical Report
Publication Date
Jun 01, 1986
Accession Number
ADA168894

Entities

People

  • John J. Fontanella
  • Mary C. Wintersgill

Organizations

  • United States Naval Academy

Tags

Communities of Interest

  • Advanced Electronics
  • C4I
  • Space
  • Weapons Technologies

DTIC Thesaurus Topics

  • Chemical Engineering
  • Chemical Synthesis
  • Chemistry
  • Elastomers
  • Electrical Conductivity
  • Glass Transition Temperature
  • High Pressure
  • Jet Propulsion
  • Macromolecules
  • Materials
  • Materials Science
  • Military Research
  • Perchlorates
  • Polymers
  • Pressure Measurement
  • Relaxation Time
  • Transition Temperature

Fields of Study

  • Materials science

Readers

  • Materials Science and Engineering.
  • Polymer Science and Engineering.