Transmission Electron Microscopy Study of Alumina Fiber-Reinforced Magnesium Composite.

Abstract

A detailed microstructral analysis of alumina (FP) fiber-reinforced ZE41A magnesium composite was performed by means of transmission electron microscopy (TEM). Fifty-five volume percent FP fiber-reinforced ZE41A magnesium composite thin foils were prepared by methods of mechanical polishing and ion thinning. Three major areas of interest in the composite microstructure were studied; the filaments, the interface (fiber/matrix reaction zone), and the matrix. In addition, the effects of heat treatments at 450 C on the composite microstructure were investigated. It was found that the alumina/magnesium interface consisted of a thin layer of magnesium aluminum oxide spinel and relatively large magnesium oxide (MgO) particles. A concentric layer of magnesium alloy grains encircling the alumina the magnesium matrix microstructures. Upon heat treatment at 450 C for 95 hours, polygonization of the magnesium matrix occurred while the spinel interfacial layer grew with decreasing magnesium oxide particle size. Keywords: Metal matrix composites, Aluminum oxides, Magnesium, Electron microscopy, Fiber Reinforced composites.

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Document Details

Document Type
Technical Report
Publication Date
Jan 01, 1987
Accession Number
ADA179912

Entities

People

  • Ernest S. Chin

Tags

Communities of Interest

  • Advanced Electronics
  • Energy and Power Technologies
  • Space
  • Weapons Technologies

DTIC Thesaurus Topics

  • Air Force
  • Alloys
  • Composite Material Fabrication
  • Composite Materials
  • Electron Microscopy
  • Heat Treatment
  • Magnesium Compounds
  • Materials
  • Materials Processing
  • Materials Science
  • Materials Testing
  • Metal Matrix Composites
  • Microscopy
  • Military Research
  • Particle Size
  • Particles
  • Transmission Electron Microscopy

Fields of Study

  • Materials science

Readers

  • Materials Science and Engineering.
  • Reinforced Composite Materials
  • Surface Engineering/Surface Coating Technology.

Technology Areas

  • Microelectronics
  • Microelectronics - Graphene