Low Pressure Compaction of SHS (Self-Propagating High-Temperature Synthesis) Prepared Ceramics.

Abstract

Titanium carbide, Titanium diboride and cermets of these compounds have been synthesized by the Self-Propagating High-Temperature Synthesis (SHS) process. It has been shown, definitively, that the mechanism of Ti+C powders reacting to form TiC is the movement of melted titanium to the solid carbon lattice. Extensive porosity in the product is caused by this movement of the titanium but additional voids are formed from the expulsion of contaminant gases during the combustion process. In order to eliminate these voids and porosity in the material, the reacted samples have been compacted up to pressures of 0.41GPA (60Kpsi) immediately after the completion of the combustion. These products have results in samples with densities greater than 95% and microhardness approaching values obtained by conventional sintering techniques. Keywords: Solid Combustion, Ceramics, Ceramics Processing, Cermets, Titanium Carbide, Titanium Diboride Carbon.

Document Details

Document Type
Technical Report
Publication Date
Mar 01, 1987
Accession Number
ADA180783

Entities

People

  • Andrus Niiler
  • Michael A. Riley

Organizations

  • Ballistic Research Laboratory

Tags

DTIC Thesaurus Topics

  • Ceramic Materials
  • Cermets
  • Combustion
  • Environmental Pollutants
  • Expulsion
  • Heat Resistant Materials
  • High Temperature
  • Materials
  • Materials Processing
  • Microhardness
  • Porosity
  • Refractory Materials
  • Sintering
  • Titanium

Fields of Study

  • Materials science

Readers

  • Rocket Propulsion.
  • Surface Engineering/Surface Coating Technology.