Synthesis and Characterization of Liquid Crystalline Polyacrylates and Polymethacrylates Containing Benzyl Ether and Diphenyl Ethane Based Mesogens.

Abstract

The synthesis and radical polymerization of a novel series of acrylates and methacrylates containing p-cyanophyenyl)-2-(p-hydroxyphenyl) ethane groups attached to the polymerizable group through aliphatic spacers containing eleven and six methylenic units is described. The resulting polymers were characterized by differential scanning calorimetry and optical polarization microscopy. All polymers exhibited enantiotropic mesomorphism. Low molar mass compounds based on benzyl ether or diphenyl ethane units exhibit only monotropic or virtual transitions. This demonstrates that the polymer effect stabilizes mesophases obtained from mesogenic units which do not contain rigid interconnecting groups.

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Document Details

Document Type
Technical Report
Publication Date
Jan 01, 1985
Accession Number
ADA183507

Entities

People

  • Chain S. Hsu
  • Virgil Percec

Organizations

  • Case Western Reserve University

Tags

Communities of Interest

  • C4I

DTIC Thesaurus Topics

  • Acetic Acid
  • Acrylates
  • Alcohols
  • Aqueous Solutions
  • Chlorides
  • Classification
  • Glass Transition Temperature
  • Hydrochloric Acid
  • Liquid Crystals
  • Measurement
  • Military Research
  • Molecular Weight
  • Phase Transformations
  • Polymers
  • Security
  • Transition Temperature
  • Transitions

Fields of Study

  • Chemistry

Readers

  • Electrochemical Engineering/ Fuel Cell Technologies
  • Polymer Science and Technology