The Feasibility of Using Solid Sorbent Packed Minitubes for the Analysis of Aqueous Organics,

Abstract

A study was conducted to determine the feasibility of analyzing trace levels of organics in water, by adsorption onto a solid sorbent packed minitube followed by thermal desorption-gas chromatographic analysis. The study included: selecting appropriate sorbents, determining the optimum thermal desorption temperature, performing wet/dry experiments, choosing the optimum drying conditions and measuring analyte breakthrough (or capacity) of the minitubes. Experimental results with methyl salicylate and Chromosorb 102 yielded breakthrough volumes in excess of 50 millimeters, indicating that this could be an extremely sensitive method for the analysis of organics in water.

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Document Details

Document Type
Technical Report
Publication Date
Jul 01, 1987
Accession Number
ADA183815

Entities

People

  • J. R. Hancock
  • M. Totland

Organizations

  • Defence Research and Development Canada

Tags

DTIC Thesaurus Topics

  • Adsorbents
  • Adsorption
  • Analytical Chemistry Techniques
  • Aqueous Solutions
  • Chemical Warfare
  • Chemical Warfare Agents
  • Chromatographic Analysis
  • Chromatographs
  • Chromatography
  • Desorption
  • Detection
  • Flow Rate
  • Gas Chromatography
  • Materials
  • Physical Properties
  • Salicylates
  • Water

Readers

  • Analytical Chemistry