Trace Analysis by MS/MS on a Double Focussing Mass Spectrometer,

Abstract

Recent advances in mass spectrometry - mass spectrometry (ms/ms) indicate that this techniques has a number of advantages over conventional methods for identification and trace analysis of organic materials (1). The method involves detection of fragment or daughter ions which arise from spontaneous or collisionally activated decomposition of parent ions in a field free region of the spectrometer. The main advantages are the additional information provided in the form of generic relationships between ions in the mass spectrum and the high specificity which can be achieved. In many cases, data obtained by ms/ms is sufficient to differentiate between isomeric structures. Although the ion intensity observed by ms/ms methods is considerably lower than with conventional MS, the reduction in 'chemical noise' is generally sufficient to allow detection of compounds at low levels by direct mixture analysis.

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Document Details

Document Type
Technical Report
Publication Date
May 01, 1987
Accession Number
ADA187954

Entities

People

  • A. G. Moritz
  • V. T. Borrett

Organizations

  • Defence Science and Technology Group

Tags

Communities of Interest

  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Acquisition
  • Alkanes
  • Data Acquisition
  • Detection
  • Electrostatic Analyzers
  • Mass Spectra
  • Mass Spectrometers
  • Mass Spectrometry
  • Mass Spectroscopy
  • Materials
  • Measurement
  • Monitoring
  • Organic Materials
  • Spectra
  • Spectrometers
  • Spectrometry
  • Spectroscopy

Fields of Study

  • Chemistry

Readers

  • Analytical Chemistry
  • Molecular Photonics/Laser Physics
  • Systems Analysis and Design