Hyaluronidase: Purification and Inhibition by a Gold Complex and a Steroid Derivative.

Abstract

The enzyme hyaluronidase from human synovial fluid was partially purified using gel filtration and chromotography on a hydroxylapatite column. A 4.1 fold purification of hyaluronidase having a specific activity of 1.1 x 10 to the minus 4th power micro mol/min/mg was obtained. The enzyme was inhibited by the gold complex Auranofin, and the steroid derivative, 22 ketocholesterol oxime. It was shown that the complexes differed in their ability to inhibit the enzyme. The rate constants and equilibrium inhibition constants were calculated. Kinetic analyses demonstrated an apparent uncompetitive inhibition by the steroid derivative 22-ketocholesterol oxime.

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Document Details

Document Type
Technical Report
Publication Date
Dec 11, 1987
Accession Number
ADA191772

Entities

People

  • Gary G. Durante

Organizations

  • Auburn University

Tags

DTIC Thesaurus Topics

  • Amino Acids
  • Arthritis
  • Blood
  • Cartilage
  • Cellular Structures
  • Chemical Synthesis
  • Chemistry
  • Connective Tissue Diseases
  • Dermatologic Agents
  • Gel Electrophoresis
  • Health Services
  • Joint Diseases
  • Joints (Anatomy)
  • Materials
  • Organic Chemistry
  • Rheumatic Diseases

Fields of Study

  • Biology

Readers

  • Molecular and Cellular Biochemistry