Synthesis of 1,4-Butanediamine-1,1,4,4-d4, 1,4-Butanediamine-2,2,3,3-d4 and Their Respective BIS (Ammonium Nitrate) Salts

Abstract

Synthesis of the title compounds from diethyl succinate and from dimethyl acetylenedicarboxylate in 16 percent overall yield, respectively, and their bis(ammonium nitrate) salts in 62 and 60 percent yields, respectively, are described. Physical properties and nuclear magnetic resonance, infrared and mass spectral data are presented.

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Document Details

Document Type
Technical Report
Publication Date
Dec 01, 1987
Accession Number
ADA194518

Entities

People

  • Alan P. Marchand
  • N. Satyanarayana
  • Robert L. Mckenney Jr.
  • Stephen R. Struck

Organizations

  • University of North Texas

Tags

Communities of Interest

  • Counter IED
  • Human Systems

DTIC Thesaurus Topics

  • Acids
  • Air Force
  • Alcohols
  • Ammonium Nitrate
  • Chemical Synthesis
  • Chemistry
  • Classification
  • Contracts
  • Elements
  • Energetic Materials
  • Mass Spectra
  • Munitions
  • Nitric Acid
  • Rocket Oxidizers
  • Security
  • Spectra
  • Water

Fields of Study

  • Chemistry

Readers

  • Organic Chemistry