The Reaction of Hydrogen with Oxygen on a Polycrystalline Iron Surface

Abstract

The Reaction of Hydrogen with Oxygen on a Polycrystalline Iron Surface, Mehran Arbab and John B. Hudson, Materials Engineering Department, Rensselaer Polytechnic Institute, Troy, NY 12180. We have studied the interaction between hydrogen and oxygen on a polycrystalline iron sample using Auger electron spectroscopy (AES) and mass spectrometry. A hydrogen permeation method was used. We found that chemisorbed oxygen cannot be removed by reaction with adsorbed hydrogen, while oxygen incorporated into the near surface region of the bulk is titrated rapidly, to leave a constant amount of (Chemisorbed) oxygen on the surface, independent of reaction temperature. All results, including both the titration data obtained by AES and the water formation and desorption rates determined by mass spectroscopy, could be interpreted with an overall activation energy of 16.0 + 2.6 Kcal/mole. Of this total energy, 8.5 + 0.4 Kcal/mole was determined to be due to the kinetics of hydrogen permeation through the iron sample. Keywords: Surfaces; Chemistry; Kinetics; Adsorption; Oxygen; Hydrogen; Metals.

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Document Details

Document Type
Technical Report
Publication Date
Feb 28, 1988
Accession Number
ADA196488

Entities

People

  • John B. Hudson
  • Mehran Arbab

Organizations

  • Rensselaer Polytechnic Institute

Tags

Communities of Interest

  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Abstracts
  • Auger Electron Spectroscopy
  • Auger Electrons
  • Chemistry
  • Contracts
  • Desorption
  • Electron Spectroscopy
  • Engineering
  • Governments
  • Heat Of Activation
  • Kinetics
  • Mass Spectrometry
  • Materials Engineering
  • Military Research
  • Spectrometry
  • Spectroscopy
  • Steady State

Fields of Study

  • Chemistry
  • Materials science

Readers

  • Electrochemical Engineering/ Fuel Cell Technologies

Technology Areas

  • Microelectronics