Design of a Scanning Tunneling Microscope for Electrochemical Applications

Abstract

We present a design for a scanning tunneling microscope that is well suited for electrochemical investigations. The construction of the microscope insures that only the tunneling tip and the sample participate in electrochemical reactions. The design also allows rapid replacement of the tip or sample, and enables facile introduction of auxiliary electrodes for use in electrochemical experiments. The microscope utilizes stepped motor driven approach mechanics in order to achieve fully remote operation and to allow reproducible coarse control of tip/sample spacings fpr electrochemical experiments. This microscope has enabled us to image highly ordered pyrolytic graphite at atomic resolution in air and aqueous solutions. Design, Electrochemistry.

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Document Details

Document Type
Technical Report
Publication Date
Oct 28, 1988
Accession Number
ADA201952

Entities

People

  • Calvin F. Quate
  • Christoph A. Lang
  • Michael J. Heben
  • Moris M. Dovek
  • Nathan S. Lewis

Organizations

  • California Institute of Technology

Tags

Communities of Interest

  • Advanced Electronics
  • Air Platforms

DTIC Thesaurus Topics

  • Brushless Dc Motors
  • Chemical Compounds
  • Chemistry
  • Construction
  • Electrochemical Cells
  • Electrochemical Reactions
  • Electrochemistry
  • Electrodes
  • Graphitic Materials
  • Liquids
  • Manufacturing
  • Mechanics
  • Microscopes
  • Military Research
  • Motors
  • Physics
  • Stepper Motors

Readers

  • Electrochemical Engineering/ Fuel Cell Technologies
  • Software Engineering
  • Thin Film Deposition Science.

Technology Areas

  • Space