Dissolution Rates of Poly(Methyl Methacrylate) in Mixtures of Non-Solvents.

Abstract

As predicted by thermodynamic studies of polymer conformation, high molecular weight poly(methyl methacrylate), PMMA, dissolves cleanly, and at a constant rate, in a 7:3 mixture of 1-butanol and acetonitrile although neither liquid is a solvent for PMMA by itself. Mixtures of other alcohols with acetonitrile also dissolve PMMA. When mixture with the same fraction of acetonitrile are compared, methanol dissolves PMMA almost twice as fast, ethanol and hexanol at about the same rate, and 2-propanol somewhat more slowly than the 1-butanol mixture with acetonitrile. The measurements of dissolution rate were made using a laser interferometer at 20 C. Keywords: Microlithography, Resists, Poly(methyl methacrylate). (aw)

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Document Details

Document Type
Technical Report
Publication Date
May 12, 1989
Accession Number
ADA207673

Entities

People

  • Francisco J. Medellı́n-Rodrı́guez
  • J.L. Sullivan
  • P. D. Krasicky
  • R. J. Groele
  • S.-w. Chun

Organizations

  • Cornell University School of Chemical and Biomolecular Engineering

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Communities of Interest

  • Advanced Electronics
  • Ground and Sea Platforms
  • Weapons Technologies

DTIC Thesaurus Topics

  • Alcohols
  • Alkenes
  • Chemical Engineering
  • Chemical Synthesis
  • Chemistry
  • Classification
  • Engineering
  • Engineers
  • Films
  • Interferometers
  • Ketones
  • Measurement
  • Methacrylates
  • Military Research
  • New York
  • Organic Chemistry
  • United States

Fields of Study

  • Chemistry

Readers

  • Organic Chemistry
  • Polymer Science and Technology

Technology Areas

  • Directed Energy
  • Directed Energy - Lasers