Negative-Working Electron Beam Resist Based on Poly(methyl methacrylate)

Abstract

Blends of polymethylmethacrylate (PMMA) and dipentaerythritol pentaacrylate (DPEPA) respond to electron beam exposure as negative resists, with sensitivity that increases with increasing DPEPA concentration. Blends of 80 wt. % PMMA and 20 wt. % DPEPA exhibit an electron sensitivity of 4 microcoulombs/sq cm and a contrast gamma of 1.2. Resolution of 0.25 micrometers has been demonstrated with this blend without the use of non-solvent rinses or plasma de-scumming. This superior resolution for a negative electron resist is attributed to the small degree of swelling of the PMMA host polymer. Increasing the molecular weight of the PMMA component to 450,000 increases the sensitivity to 1 microcoulomb/sq cm improves the contrast to a gamma value of 2.3 without affecting resolution or sensitivity relative to the blends with low molecular weight PMMA.

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Document Details

Document Type
Technical Report
Publication Date
May 12, 1989
Accession Number
ADA207834

Entities

People

  • B. C. Dems
  • Francisco J. Medellı́n-Rodrı́guez
  • S. K. Obendorf
  • Y. M. Namastet

Organizations

  • Cornell University School of Chemical and Biomolecular Engineering

Tags

Communities of Interest

  • Ground and Sea Platforms

DTIC Thesaurus Topics

  • Abstracts
  • Alkenes
  • Chemical Engineering
  • Chemical Synthesis
  • Chemistry
  • Chromatographs
  • Contrast
  • Electron Beams
  • Electrons
  • Films
  • High Resolution
  • Liquid Chromatography
  • Methacrylates
  • Microlithography
  • Military Research
  • Molecular Weight
  • Sensitivity

Readers

  • Mathematics or Statistics
  • Nanofabrication and Microfabrication.
  • Polymer Science and Engineering.

Technology Areas

  • Directed Energy
  • Directed Energy - Lasers
  • Microelectronics
  • Microelectronics - Graphene