Monolayers of 11-Trichlorosilylundecyl Thioacetate: A System that Promotes Adhesion Between Silicon Dioxide and Evaporated Gold

Abstract

This chapter describes the use of sulfur-containing organic monolayers to improve the adhesion of gold to silicon substrates having a native silicon dioxide surface layer. Gold adheres to clean silicon, but not to silicon dioxide. The affinity of gold toward silicon dioxide can be improved by coating with chromium or titanium films or by adding interlayers containing fluoride salts. Bombardment of gold-covered silicon dioxide with electrons or heavy ions also enhances adhesion. Thin covalently-bonded alkylsiloxane films containing amines or epoxides improve the adherence of gold to glass. Here we demonstrate that covering a Silicon/Silicon dioxide substrate with a covalently attached organic monolayer film containing thiol groups (and possibly disulfides derived from them) or thioacetate groups improves the adhesion of gold to the substrate.

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Document Details

Document Type
Technical Report
Publication Date
May 01, 1989
Accession Number
ADA208266

Entities

People

  • George M. Whitesides
  • Hans Biebuyck
  • Stephen R. Wasserman

Organizations

  • Harvard University

Tags

Communities of Interest

  • Advanced Electronics

DTIC Thesaurus Topics

  • Abstracts
  • Adhesion
  • Chemical Engineering
  • Chemical Synthesis
  • Chemistry
  • Chlorides
  • Composite Materials
  • Engineering
  • Failure Mode And Effect Analysis
  • High Resolution
  • Materials
  • Materials Laboratories
  • Materials Science
  • Measurement
  • Military Research
  • Silicon Dioxide
  • Universities

Readers

  • Organic Chemistry
  • Thin Film Deposition Science.

Technology Areas

  • Microelectronics
  • Microelectronics - Graphene