Solid Lubrication Studied by Optical Means

Abstract

The well-known and unwelcome phenomenon of the formation of carbon or coke on the surfaces of some clay and clay-supported transition metal cracking and dehydrogenation catalysts used in petroleum refining was applied to developed a process for the lubrication of tribo-surfaces at high temperatures by continuously regenerated surface carbon derived from flow of ethylene gas. Measurements with a pin-on-disc tribometer showed an immediate reduction of friction (from as high as 0.6 to as low as 0.05) and wear for nickel, palladium, ceramics coated with these metals and for bare silicon carbide and nitride at temperatures between 400 and 650 C and 0.2 MPa average Hertzian pressures, as soon as ethylene was introduced into the conjunction region. The environment could be air under ambient conditions. The carbon deposits were analyzed by Auger and Raman spectroscopy and ellipsometry and found to be generally about 400 A thick and microcrystalline graphite or vitreous.

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Document Details

Document Type
Technical Report
Publication Date
Mar 31, 1989
Accession Number
ADA209008

Entities

People

  • James L. Lauer

Organizations

  • Rensselaer Polytechnic Institute

Tags

Communities of Interest

  • Advanced Electronics

DTIC Thesaurus Topics

  • Alkenes
  • Aluminum Oxides
  • Auger Electron Spectroscopy
  • Auger Electrons
  • Ceramic Materials
  • Chemistry
  • Electron Spectroscopy
  • Friction
  • High Temperature
  • Lubricants
  • Lubrication
  • Measurement
  • Raman Spectroscopy
  • Silicon Carbide
  • Spectra
  • Spectroscopy
  • Transition Metals

Fields of Study

  • Materials science

Readers

  • Organic Chemistry
  • Thin Film Deposition Science.
  • Tribology (the study of the boundary interaction between sliding surfaces, lubrication, wear and friction).