Nuclear Magnetic Resonance Signatures of Nitrogen-Containing Compounds

Abstract

Experiments were conducted to determine if unique NMR signatures can be detected and defined for the proton NMR signals of nitrogen-containing compounds. Compounds of particular interest include explosives and explosive stimulants. The effects of off resonance radio frequency (rf) irradiation or pumping in three were observed in three nitrogen-containing compounds: HMT, TNT, and PETN. Similar effects were observed in mannitol and in the plastic explosive C-4 but dielectric heating of the sample C-4 made it impossible to apply the required sequence of rf pulses. The NMR FID signal from C-4 contains two distinct components. At present, methods to enhance the effects of off-resonance irradiation and improve the NMR signature are not obvious. With proper design, it may be possible to take advantage of the observed effects in field-usuable NMR explosive detectors. Keywords: Nuclear magnetic resonance; Free induction decay; Hexamethylenetetramine; Mannitol; Larmor frequency; Trinitrotoluene; Pentaerythritol tetranitrate.

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Document Details

Document Type
Technical Report
Publication Date
Aug 01, 1989
Accession Number
ADA213375

Entities

People

  • J. P. Sanders
  • L. J. Burnett
  • M. A. Fineman

Organizations

  • University of California, San Diego

Tags

Communities of Interest

  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Detection
  • Detectors
  • Energy Levels
  • Explosives
  • Explosives Detection
  • Frequency Bands
  • Magnetic Fields
  • Magnetic Moments
  • Magnetic Resonance
  • Materials
  • Nuclear Magnetic Resonance
  • Nuclei
  • Observation
  • Plastic Explosives
  • Quantum Properties
  • Radio Frequency
  • Radio Frequency Pulses

Fields of Study

  • Physics

Readers

  • Agricultural Chemistry/Soil Science
  • Analytical Chemistry
  • Pulsed Power and Plasma Physics.