A Preliminary Assessment of 3-Nitro-1,2,4-Triazol-5-One (NTO) as an Insensitive High Explosive

Abstract

A simple two-step method to produce NTO in high yield from semicarbazide hydrochloride has been defined. A free-flowing material with bulk density more than 0.9 g/ml has been produced by stirred aqueous recrystallisation; surfactants were ineffective in altering crystal habit. Impact sensitiveness of NTO was higher than expected although apparent propagation ability is low. Ignitability under thermal and electrostatic stimuli is substantially lower than RDX. Experimental firings were conducted to assess explosive performance for charges pressed to about 90% TMD; velocity of detonation at 12.7 mm and 15.9 mm diameter was determined while detonation pressure (plate dent) and critical diameter were estimated. Performance at these diameters is somewhat lower than RDX. Moulding powders for 95:5 NTO/binder formulations were prepared from three commercial EVA resins and a flame retardant polyphosphazene. All three NTO/EVA formulations were insensitive to impact. Recommendations for continuing studies on insensitive booster formulations have been made.

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Document Details

Document Type
Technical Report
Publication Date
Jul 01, 1989
Accession Number
ADA215063

Entities

People

  • C. N. Louey
  • M. G. Wolfson
  • R. J. Spear

Organizations

  • Defence Science and Technology Group

Tags

Communities of Interest

  • Weapons Technologies

DTIC Thesaurus Topics

  • Chemical Synthesis
  • Chemistry
  • Detonations
  • Explosions
  • Explosives
  • Flame Retardants
  • Fluids
  • High Explosives
  • Ignition
  • Insensitive Explosives
  • Materials
  • Materials Laboratories
  • Materials Science
  • Measurement
  • Microscopy
  • Munitions
  • Organic Chemistry

Readers

  • Analytical Chemistry
  • Polymer Science and Engineering.
  • Rocket Propulsion.