Quartz Crystal Microbalance Study: Ionic Motion Across Conducting Polymers

Abstract

In-situ monitoring of mass change was performed during electro chemical growth and redox cycling of a conducting polymer (polypyrrole) on a quartz crystal microbalance. For the polypyrrole films grown with large polymeric anions (poly(4-styrenesulfonate) and poly-vinylsulfonate), mostly cations and solvent molecules were inserted and removed to compensate charge in polypyrrole. The films formed with medium sized anions (tosylate) showed both anion and cation motion during the redox process. The films prepared in the presence of small anions (clo4(-) and BF4(1) showed mostly anion motion, but cation motion also became significant for higher oxidation and/or reduction rate. (kr)

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Document Details

Document Type
Technical Report
Publication Date
Mar 15, 1990
Accession Number
ADA221079

Entities

People

  • Mary Lien
  • Naoi Katsuhiko
  • William H. Smyrl’

Organizations

  • University of Minnesota

Tags

Communities of Interest

  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Acetonitrile
  • Chemical Engineering
  • Chemistry
  • Computers
  • Conductive Polymers
  • Electrochemical Reactions
  • Electrodes
  • Frequency
  • Frequency Shift
  • Materials Science
  • Measurement
  • Microbalances
  • Military Research
  • Nitriles
  • Personal Computers
  • Polymeric Films
  • Quartz Crystal Microbalances

Fields of Study

  • Chemistry

Readers

  • Electrochemical Engineering/ Fuel Cell Technologies
  • Electrochemical Surface Science
  • Thin Film Deposition Science.