Poly(p-phenyleneterephthalamide propanesulfonate): a New Polyelectrolyte for Application to Conducting Molecular Composites

Abstract

A new water soluble polyelectrolyte has been synthesized by the alkyl sulfonation of the aramid poly-(p-phenyleneterephthalamide) (PTTA) to form poly(p-phenyleneterephthalamide propanesulfonate) (PPTA-PS). This polyelectrolyte is soluble in water to greater than 18% by weight when the poly- aramid is alkyl sulfonated to 66%. Characterization and structural analysis of the polyelectrolyte was facilitated by a Carbon 13 Nuclear Magnetic Resonance study of the model compound benzanilide and its alkyl and alkyl sulfonate derivatives, as well as of an alkyl derivative of PPTA. The preparation of a molecular level composite of polypyrrole and PPTA-PS has been pursued by electrochemical polymerization of pyrrole using PPTA-PS as both the electrolyte and the polymeric dopant ion. The composite materials exhibit conductivities of 1 ohm/cm and improved thermal stabilities when compared to poly(pyrrole tosylate). (KT)

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Document Details

Document Type
Technical Report
Publication Date
Apr 17, 1990
Accession Number
ADA221082

Entities

People

  • John R. Reynolds
  • Melinda B. Gieselman

Organizations

  • University of Texas at Arlington

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  • Advanced Electronics

DTIC Thesaurus Topics

  • Aqueous Solutions
  • Chemical Shifts
  • Chemical Synthesis
  • Chemistry
  • Composite Materials
  • Conductive Polymers
  • Conductivity
  • Electrodes
  • Electrolytes
  • Films
  • Macromolecules
  • Materials
  • Materials Science
  • Organic Chemistry
  • Polymers
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  • United States

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  • Chemistry
  • Materials science

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  • Polymer Science and Technology
  • Reinforced Composite Materials