PH3 Surface Chemistry on Si(111)-(7x7) A Study by Auger Spectroscopy and Electron Stimulated Desorption Methods

Abstract

The adsorption and decomposition of phosphine hydride on silicon (III)-(7x7) was investigated in ultrahigh vacuum by means of temperature programmed desorption (TPD), low-energy electron diffraction (LEED), Auger electron spectroscopy (AES) and electron stimulated desorption (ESD) methods. Phosphine adsorbs on Si(III)-(7x7) at T=120K with an initial sticking coefficient of S(o) equivalent to 1 through a mobile (extrinsic) precursor state. Some PH3 dissociative adsorption at 120 K is observed. Thermal activation of the adsorbed species results in desorption of a molecular PH3 species up to 550 K. Further heating produces H2(g) desorption at T equivalent to 740 K and P2(g) desorption at T equivalent to 1010 K, thus indicating that PH3 decomposition has occurred. AES and ESD studies of the adsorbed species reveal that decomposition takes place by the breaking of P-H bonds in PHx(a) to form Si-H species on the surface for 120 K < T < 700 K. Keywords: Si (III); PH3; Phosphine; Phosphorus; Adsorption; Silicon; Doping; Chemical vapor deposition; Passivation; Semiconductors; Crystal growth.

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Document Details

Document Type
Technical Report
Publication Date
Apr 11, 1990
Accession Number
ADA221508

Entities

People

  • J. T. Yates Jr.
  • P. A. Taylor
  • R. M. Wallace
  • Wolfgang J. Wolfgang J. Choyke

Organizations

  • University of Pittsburgh

Tags

Communities of Interest

  • Energy and Power Technologies
  • Ground and Sea Platforms
  • Weapons Technologies

DTIC Thesaurus Topics

  • Auger Electron Spectroscopy
  • Auger Electrons
  • Chemical Vapor Deposition
  • Chemistry
  • Electron Beams
  • Electron Energy
  • Electron Guns
  • Electron Spectroscopy
  • Electrons
  • Ionization
  • Mass Spectrometers
  • Measurement
  • Military Research
  • Spectra
  • Spectroscopy
  • Surface Chemistry
  • Temperature Gradients

Readers

  • Electrochemical Engineering/ Fuel Cell Technologies
  • Thin Film Deposition Science.

Technology Areas

  • Microelectronics
  • Microelectronics - Graphene