Metallurgical Analysis of Leaking Tray Packs

Abstract

A metallurgical analysis was performed to determine the cause of leaking tray packs and the origin and development of 'gray spots' which represent potential leak sites. Tray packs are fabricated of tin-free steel (TFS) and are protected with multilayered coatings on both interior and exterior surfaces. Accelerated corrosion tests were carried out in order to monitor the progress of corrosion in a simulated long-term exposure environment. The presence of 'gray spots' on the exterior surface of the tray packs was related to an existing defect in the directly opposite surface of the interior coatings. Microscopic examination, in conjunction with AC impedance measurements, showed that water and aggressive ions contained in the food penetrate into and through interior coatings, through localized defects such as pores and cracks, causing pitting of the TFS which intensifies as a result of the presence of an occluded electrochemical cell at the coating/metal interface. Once the pit has penetrated through the entire thickness of the TFS, a gray spot appears under the exterior clear epoxy coating.

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Document Details

Document Type
Technical Report
Publication Date
May 01, 1990
Accession Number
ADA223157

Entities

People

  • Frank C. Chang
  • Kuan S. Lei
  • Milton Levy

Tags

Communities of Interest

  • Advanced Electronics

DTIC Thesaurus Topics

  • Coatings
  • Corrosion Resistance
  • Electrical Measurement
  • Electrochemical Reactions
  • Electron Microscopy
  • Engineering
  • Environment
  • Epoxy Coatings
  • Frequency
  • Information Processing
  • Materials
  • Microscopes
  • Microscopy
  • Military Research
  • Organic Coatings
  • Scanning Electron Microscopy
  • Sodium Compounds

Readers

  • Battery Technology and Engineering
  • Surface Coatings Technology.
  • Surface Engineering/Surface Coating Technology.