Complex Formation between Dimethyl Methylphosphonate and Hexafluoroisopropanol

Abstract

A solvent/water partitioning method was used to measure the complex formation between dimethyl methylphosphonate (DMMP) and hexafluoroisopropanol (HFIP). The highest formation constant was obtained when n-hexane was used as the partitioning solvent. Other solvents all interfered to some extent with complex formation, probably by interacting with HFIP. The log formation constant in carbon tetrachloride was 3.46 + or - 0.10 at 21 C, which was similar to literature estimates for other phosphonates. The data support formation of H- bond charge transfer complexes as the mechanism for HFIP interaction with phosphonates and as primarily responsible for HFIP extraction of these compounds from water. Keywords: Complexation, Dimethyl methylphosphonate (DMMP), Hexafluoroisopropanol (HFIP).

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Document Details

Document Type
Technical Report
Publication Date
Jun 01, 1990
Accession Number
ADA226221

Entities

People

  • Daniel C. Leggett

Organizations

  • Cold Regions Research and Engineering Laboratory

Tags

Communities of Interest

  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Analytical Chemistry
  • Carbon Tetrachloride
  • Chemical Compounds
  • Chemical Synthesis
  • Chemical Warfare Agents
  • Chemistry
  • Cold Regions
  • Engineering
  • Esters
  • Extraction
  • Free Energy
  • Literature
  • Methylphosphonates
  • Phase
  • Phosphonates
  • Polymers
  • Solvent Extraction

Fields of Study

  • Chemistry

Readers

  • Analytical Chemistry
  • Organic Chemistry