Isolation and Characterization of the Arsorane (Me3SiCH2)3AsCl2

Abstract

Our research involving the preparation of gallium-arsenic compounds has required a variety of specific new organoarsenic starting materials, including primary and secondary arsines; thus, certain synthetic procedures have had to be developed in our laboratories to meet these needs. Of course, all of the attempts to synthesize desired materials were not productive and, at times, side reactions were significant. (js)

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Document Details

Document Type
Technical Report
Publication Date
Sep 21, 1990
Accession Number
ADA227001

Entities

People

  • A. P. Purdy
  • C. G. Pitt
  • R. L. Wells

Organizations

  • Duke University

Tags

DTIC Thesaurus Topics

  • Abstracts
  • Barometric Pressure
  • Chemical Laboratories
  • Chemical Synthesis
  • Chemistry
  • Controlled Atmospheres
  • Electrons
  • Filtration
  • Mass Spectra
  • Mass Spectrometers
  • Mass Spectrometry
  • Measurement
  • Melting Point
  • Military Research
  • Spectra
  • Spectrometry
  • Spectroscopy

Readers

  • Organic Chemistry
  • Systems Analysis and Design

Technology Areas

  • Microelectronics