Model Filled Polymers versus Synthesis of Crosslinked Monodisperse Polymethacrylate Beads

Abstract

Monodisperse polymethacrylate beads of varied size and crosslink density are prepared by emulsion copolymerization of methacrylate and divinyl monomers in the absence of emulsifiers. The sizes of polybutyl and polyethyl methacrylate beads decreased with increasing polymerization temperature, while polymethyl methacrylate beads were largely unchanged in size. The molar mass of polymer in polymethyl methacrylate beads markedly exceeded that in polystyrene beads. The rate of polymerization increased, and bead size decreased, with increasing initiator concentration or decreasing monomer concentration. The polymethacrylate beads are used as filler particles in polymer composites. Keywords: Polymer beads; Crosslinked monodisperse beads; Polymethacrylates; Filled polymers.

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Document Details

Document Type
Technical Report
Publication Date
Sep 25, 1990
Accession Number
ADA227236

Entities

People

  • D. Zou
  • Liuyang Sun
  • M. Park
  • R. Guan
  • Shuo Ma

Organizations

  • University of Southern California

Tags

Communities of Interest

  • Weapons Technologies

DTIC Thesaurus Topics

  • Alkenes
  • California
  • Chemical Engineering
  • Chemical Synthesis
  • Chemistry
  • Engineering
  • Ethylene Glycol
  • Ethylenes
  • Glycols
  • Military Research
  • Molecular Weight
  • Particle Size
  • Polymer Chemistry
  • Polymers
  • Polymethyl Methacrylate
  • Reaction Time
  • United States

Fields of Study

  • Chemistry

Readers

  • Aerosol Science/Aerosol Physics
  • Polymer Science and Technology