In situ Vibrational Spectroscopy of Contact Adsorbed Thiocyanate on Silver Electrodes: Experiment and Theory

Abstract

In-situ FT-IR vibrational spectra of thiocyanate ions absorbed on polycrystalline Ag electrodes as a function of electrode potential and electrolyte concentration are reported. Interpretation of the results are performed with the help of ab initio SCF calculations of the electronic structure and bonding of thiocyanate to small silver clusters. It was concluded that thiocyanate ion adsorbs with S- N-end down in the double layer region for potentials greater than -0.3V (versus Ag/AgCl). At potentials close to the potential of zero charge thiocyanate ion is absorbed flat and cannot be detected by IR.

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Document Details

Document Type
Technical Report
Publication Date
Jan 01, 1987
Accession Number
ADA229750

Entities

People

  • G. Pacchioni
  • H. Seki
  • K. Kunimatsu
  • M. R. Philpott
  • Mahesh G. Samant
  • P. S. Bagus
  • R. Viswanathan

Organizations

  • International Business Machines Corporation (Armonk, NY)

Tags

Communities of Interest

  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Adsorption
  • California
  • Chemical Synthesis
  • Chemistry
  • Crystal Structure
  • Electric Fields
  • Electrolytes
  • Frequency
  • Geometry
  • Military Research
  • Orientation (Direction)
  • Polycrystals
  • Potential Energy
  • Spectra
  • Spectroscopy
  • Two Dimensional
  • Vibrational Spectra

Readers

  • Electrochemical Engineering/ Fuel Cell Technologies
  • Molecular Photonics/Laser Physics

Technology Areas

  • Microelectronics