Synthesis of Organic Compounds (Selected Articles)

Abstract

Synthesis is realized in essence as described for ethyl- orthotitanate. Into a three-necked round-bottomed flask with a capacity of 500 ml equipped with dropping funnel, reflux condenser and tube for the introduction of ammonia, are placed 102 g (1.75 g-mols) of thoroughly dried out allyl alcohol, which boils at 96-97 and 250 ml of absolute benzene (see note). Cooler and dropping funnel are connected with the drying tubes. From dropping funnel during cooling of reaction flask by ice water gradually during 30-40 min. are added 60 g (o.32 g-mols) of titanium tetrachloride, after which reaction mixture is saturated by dry ammonia before the achievement of increase in weight not less than 25 g (1.46 g-mols). Is filtered out the fallen ammonium chloride.

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Document Details

Document Type
Technical Report
Publication Date
Oct 03, 1990
Accession Number
ADA229903

Entities

Organizations

  • National Air and Space Intelligence Center

Tags

DTIC Thesaurus Topics

  • Alkenes
  • Barometric Pressure
  • Boiling
  • Boiling Point
  • Chlorides
  • Distillation
  • Filters
  • Foreign Technology
  • Graphics
  • Machine Translation
  • Moisture
  • Organic Compounds
  • Orthoesters
  • Titanium
  • Translations

Readers

  • Mathematics or Statistics
  • Organic Chemistry
  • Thermal Physics or Thermal Science.