Hierarchically-Clustered Structures: Formation During Colloidal Processing and Evolution During Sintering

Abstract

The research presented in this report examined the formation and microstructural evolution of colloidally consolidated systems during sintering. The microstructural evolution of a hierarchically-clustered system was treated as a whole. The main goals were (i) to develop a methodology for predicting the evolution of hierarchically-clustered structures during densification and (ii) to develop experimental techniques for modifying the hierarchical structures through colloidal consolidation techniques. Experimental and theoretical modeling studies showed that all powder compacts eventually approach a steady- state grain-size distribution regardless of the original state of the colloidally consolidated compact. During densification, all microstructures followed unique paths dependent upon the initial state of the colloidal dispersion (dispersed or flocculated suspensions), but the final microstructure always approached an equilibrium distribution independent of the initial state of the colloidal dispersion (dispersed or flocculated suspensions), but the final microstructure always approached an equilibrium independent of the initial state.

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Document Details

Document Type
Technical Report
Publication Date
Dec 04, 1990
Accession Number
ADA230704

Entities

People

  • I. A. Aksay
  • R. Kikuchi

Organizations

  • University of Washington

Tags

Communities of Interest

  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Chemical Synthesis
  • Chemistry
  • Elastic Properties
  • Heat Energy
  • Materials
  • Materials Laboratories
  • Materials Processing
  • Materials Science
  • Materials Testing
  • Mechanical Properties
  • Mechanical Working
  • Mechanics
  • Phase Diagrams
  • Phase Transformations
  • Thermodynamics
  • Three Dimensional
  • Two Dimensional

Readers

  • Aerosol Science/Aerosol Physics
  • Computational Fluid Dynamics (CFD)
  • Electrochemical Engineering/ Fuel Cell Technologies