The Effect of Post-Cure and Antimony Trioxide Addition on the Glass Transition of Polyester and Vinyl Ester Resin Systems

Abstract

The effect of post-curing on the glass transition temperature (Tg) of a variety of styrene cross-linked polyester and vinyl ester resins was determined by monitoring the changes to Tg using a Differential Scanning Calorimeter. The effect of adding the inorganic fire-retardant, antimony trioxide, on the Tg of these resin systems was also investigated. Results indicated that the effect of post-curing was to increase the amount of cross-linking of the polyester and vinyl ester resins, as evident by the beneficial increase in the glass transition temperature and changes to the storage modulus. The addition of up to 10 parts per hundred resin (phr) of the fire-retardant, antimony trioxide, had a negligible effect on the onset of the glass transition point.

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Document Details

Document Type
Technical Report
Publication Date
Dec 01, 1990
Accession Number
ADA232523

Entities

People

  • I. A. Keough
  • J. G. Dwyer
  • R. M. Morchat

Organizations

  • Defence Research and Development Canada

Tags

Communities of Interest

  • C4I
  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Antimony
  • Calorimeters
  • Glass
  • Glass Fiber Reinforced Plastics
  • Glass Transition Temperature
  • Heat Energy
  • Materials
  • Mechanical Properties
  • Physical Properties
  • Plastics
  • Polymers
  • Reinforced Plastics
  • Resins
  • Thermal Properties
  • Thermosetting Plastics
  • Transition Temperature
  • Transitions

Fields of Study

  • Materials science

Readers

  • Polymer Science and Engineering.