A Glow Discharge Ion Source with Fourier Transform Ion Cyclotron Resonance Mass Spectrometric Detection

Abstract

A glow discharge ion source has been coupled to a Fourier transform ion cyclotron resonance mass spectrometer using a series of four electrostatic lenses to accelerate and focus ions generated external to the instrument's high magnetic field into its analyzer cell. Like other glow discharge mass spectrometers, glow discharge-Fourier transform ion cyclotron resonance can provide a quantitative measure of bulk analyte concentration with good precision and accuracy. Although detection limits currently attainable are several orders of magnitude higher than the commercially available magnetic sector based instrument, this approach holds promise for ultra high mass/ultra high resolving power mass analysis. Several schemes are proposed to lower the detection limits of the technique while still providing high enough resolution to resolve isobaric interferences.

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Document Details

Document Type
Technical Report
Publication Date
May 10, 1991
Accession Number
ADA235575

Entities

People

  • Christopher M. Barshick
  • John R. Eyler

Organizations

  • University of Florida

Tags

Communities of Interest

  • Advanced Electronics
  • Weapons Technologies

DTIC Thesaurus Topics

  • Chemistry
  • Cyclotron Resonance
  • Cyclotrons
  • Detection
  • Glow Discharges
  • High Resolution
  • Instrumentation
  • Ion Sources
  • Mass Spectra
  • Mass Spectrometers
  • Mass Spectrometry
  • Measurement
  • Military Research
  • Resonance
  • Spectra
  • Spectrometers
  • Spectrometry

Fields of Study

  • Chemistry
  • Physics

Readers

  • Analytical Chemistry
  • Plasma Physics / Magnetohydrodynamics
  • Pulsed Power and Plasma Physics.