Photoluminescence Studies of Silver-Exchanged Cadmium Selenide Crystals. Modification of a Chemical Sensor for Aniline Derivatives by Heterojunction Formation

Abstract

Single-crystal n-CdSe surfaces have been modified by an exchange reaction with aqueous Ag+ that converts part of the surface to Ag2Se and releases Cd2+ to solution. Formation of Ag2Se is established by X-ray powder diffraction. ESCA and Auger spectroscopy are consistent with the formation of Ag2Se islands having thicknesses of 0-500 A, depending on reaction conditions. Steady-state photoluminescence (PL) experiments show that Ag+-exchanged CdSe (CdSe/Ag+) can be superior to CdSe as an aniline sensor: ring-substituted aniline derivatives in toluene solution cause enhancements of the CdSe band edge PL in CdSe/Ag+ samples relative to a toluene ambient, with the effect about twice as large as for unexchanged CdSe. The variations in PL intensity of CdSe/ Ag+ are well fit by a dead-layer model, allowing estimation of the adduct- induced change in depletion width.

Open PDF

Document Details

Document Type
Technical Report
Publication Date
May 20, 1991
Accession Number
ADA236000

Entities

People

  • Arthur B. Ellis
  • Larry K. Leung
  • Ned Tabatabaie
  • Norma J. Komplin

Tags

Communities of Interest

  • Energy and Power Technologies
  • Sensors
  • Weapons Technologies

DTIC Thesaurus Topics

  • Amines
  • Chemical Detectors
  • Chemistry
  • Conduction Bands
  • Cross Domain
  • Diffraction
  • Energy Bands
  • Equations
  • Fermi Levels
  • Military Research
  • Organic Chemistry
  • Photoelectrons
  • Physical Chemistry
  • Relaxation Time
  • Single Crystals
  • Spectra
  • Spectroscopy

Readers

  • Materials Science and Engineering.
  • Organic Chemistry