New Polymer Electrolyte Hosts and Their Tetrabutylammonium Chloride Complexes. Relationships Among Concentration of Polar Groups, ESR Spin Probe Response, and Ionic Conductivity.

Abstract

A new polymer electrolyte host was synthesized by hydrosilation of a poly(hydromethylsiloxane) with terminal olefin bearing a silyl ketene acetal. The derivatized siloxane was subsequently reacted with 4-nitrobenzenesulfenyl chloride, affording polymers having highly polar pendants. Complexes of these polymers with tetrabutylammonium chloride were prepared. The ionic conductivities of these materials are a function of concentration of polar pendent groups and, as a result, the glass transition temperature. The weak dependence of polymer host Tg on tetrabutylammonium chloride concentration makes these ideal model systems to explore the factors which ultimately limit ionic conductivity.

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Document Details

Document Type
Technical Report
Publication Date
Jun 12, 1991
Accession Number
ADA240497

Entities

People

  • Chia-yu Yang
  • Gary E Wnek

Organizations

  • Rensselaer Polytechnic Institute

Tags

Communities of Interest

  • Advanced Electronics
  • Sensors

DTIC Thesaurus Topics

  • Alkali Metals
  • Charge Carriers
  • Chemistry
  • Chlorides
  • Conductivity
  • Diffraction
  • Electron Spin Resonance
  • Frequency
  • Glass
  • Glass Transition Temperature
  • Heat Of Activation
  • Materials
  • Military Research
  • Polymers
  • Spectra
  • Spin Resonance
  • Transition Temperature

Fields of Study

  • Chemistry
  • Materials science

Readers

  • Electrochemical Engineering/ Fuel Cell Technologies
  • Organic Chemistry
  • Polymer Science and Technology