Electrochemical and Scanning Tunneling Microscopic Study of Dealloying of Cu3Au

Abstract

Dealloying of Copper gold alloys has been examined by in-situ STM and several electrochemical methods. Three different regimes of behavior were noted. At low overpotentials, clustering of gold atoms occurs near sites of copper dissolution. This is essentially a two-dimensional process. The formation and smoothing of these clusters by capillary action, monitored in real time, demonstrated the highly mobile nature of the surface species. At higher potentials, the electrode is largely passivated by the enrichment of gold. However, there exist small localized regions of three-dimensional roughness which may be correlated to extended dealloying catalyzed by bulk solid-state defects.

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Document Details

Document Type
Technical Report
Publication Date
Sep 20, 1991
Accession Number
ADA241140

Entities

People

  • Allen J. Bard
  • Fu-ren F. Fan
  • Thomas P. Moffat

Organizations

  • University of Texas at Austin

Tags

DTIC Thesaurus Topics

  • Alloys
  • Chemistry
  • Classification
  • Dealloying
  • Electron Microscopy
  • Elements
  • Materials
  • Melting Point
  • Microscopy
  • Phase Transformations
  • Quantum Tunneling
  • Scanning
  • Security
  • Solid Solutions
  • Stress Corrosion
  • Surface Transportation
  • Tunneling

Readers

  • Electrochemical Engineering/ Fuel Cell Technologies
  • Materials Science and Engineering.
  • Nanoscale Plasmonic Nanotechnology