Reconstruction at Ordered Au(110)-Aqueous Interfaces as Probed by Atomic-Resolution Scanning Tunneling Microscopy

Abstract

Atomic resolution scanning tunneling microscopy (STM) images of ordered Au(110) in aqueous 0.1 M HC104, reported as a function of electrode potential, provide an unusually detailed picture of surface reconstruction. Lowering the potential of a freshly annealed surface to -0.3 V vs SCE yield images consisting primarily of domains having (1 x 2) symmetry. While the (1 x 2) structure exhibits an atomic density commensurate with the usual missing row model, the images suggest that significant relaxation of both top- and second- layer atoms occurs. Three-atom wide ribbons, lying along the (110) direction, are seen to provide the basic building blocks of the reconstruction; these units also yield added row domains of (1 x n) symmetry, where n=3 or higher. The reconstruction is lifted, yielding the (1x1) Au(110) surface, rapidly (within ca 2s) upon altering the potential to O V vs SCE, yet reappears immediately upon returning to -0.3 V.

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Document Details

Document Type
Technical Report
Publication Date
Oct 01, 1991
Accession Number
ADA241801

Entities

People

  • A. Hamelin
  • Michael J. Weaver
  • Xiangyu Gao

Organizations

  • Purdue University

Tags

Communities of Interest

  • Materials and Manufacturing Processes

DTIC Thesaurus Topics

  • Atoms
  • Chemistry
  • Classification
  • Diffraction
  • Electrodes
  • Electron Diffraction
  • Electron Microscopy
  • Kinetic Energy
  • Metals
  • Microscopes
  • Microscopy
  • Military Research
  • Scattering
  • Security
  • Symmetry
  • X Rays
  • X-Ray Diffraction

Fields of Study

  • Physics

Readers

  • Electrochemical Surface Science
  • Mathematics or Statistics
  • Thin Film Deposition Science.