Resonant Acoustic Determination of Complex Elastic Moduli

Abstract

An acoustic resonance based technique using a free-free bar has been extended to investigate the complex (storage and loss) moduli of non-magnetic materials having circular cross section. Using this technique, the bar can be selectively excited in three independent vibrational modes, i.e., torsional, flexural, and longitudinal modes. The torsional mode yields the shear modulus. Either the flexural or longitudinal modes can be used to obtain Young's modulus. These resonant modes can be tracked continuously by means of a phase-locked-loop (PLL) as the temperature (and resonant frequency) of the rod is changed. The in- phase amplitude of the receiver output of the electrodynamic transducer is proportional to the quality factor, Q, of the material. It can be used to continuously track the loss tangent (=1/Q) of the material as a function of temperature and frequency. Results for complex shear modulus and Young's modulus were obtained for a castable epoxy type PR1592 and complex shear modulus for polymethyl methacrylate (PMMA) and Uralite 3130. Over the temperature and frequency range that was accessible, a clear viscoelastic transition was observed in both the storage modulus and loss tangent curves of PR1592.

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Document Details

Document Type
Technical Report
Publication Date
Mar 01, 1991
Accession Number
ADA245058

Entities

People

  • Beng H. Tan

Organizations

  • Naval Postgraduate School

Tags

Communities of Interest

  • Advanced Electronics
  • Biomedical
  • C4I
  • Energy and Power Technologies
  • Sensors
  • Space

DTIC Thesaurus Topics

  • Biomedical And Dental Materials
  • Computer Programs
  • Computers
  • Elastic Properties
  • Frequency Shift
  • Materials Laboratories
  • Materials Processing
  • Materials Science
  • Materials Testing
  • Measurement
  • Mechanical Working
  • Modulus Of Elasticity
  • Physical Properties
  • Resins
  • Resonant Frequency
  • Shear Modulus
  • Test Methods

Readers

  • Polymer Science and Engineering.
  • Structural Dynamics.