Chemistry of Organoindium Hydrides. The Synthesis, Characterization and Crystal Structure of K(H(In(CH2CMe3)3)2)

Abstract

Two new organoindium hydrides have been prepared and fully characterized according to their physical properties, partial elemental analyses, molecular weight studies and IR and 1H and 13C NMR spectral studies. The unique hydrogen atoms bonded to indium in the two compounds provide characteristic infrared bands and 1H NMR resonances which have been identified by comparative studies with the corresponding deuterium derivatives. Compounds which contain indium hydrogen bonds are difficult to prepare, isolate and fully characterize. Thus, no indium hydride has been fully characterized previously by elemental analyses, molecular weight studies, diagnostic spectroscopic data and an X-ray structural study.

Open PDF

Document Details

Document Type
Technical Report
Publication Date
Jan 21, 1992
Accession Number
ADA245204

Entities

People

  • Melvyn Rowen M.R. Churchill
  • O. T. Beachley Jr.
  • Ronald F. See
  • Sun-hua Chao

Organizations

  • University at Buffalo

Tags

Communities of Interest

  • Weapons Technologies

DTIC Thesaurus Topics

  • Alkanes
  • Chemical Synthesis
  • Chemistry
  • Crystal Structure
  • Crystals
  • Deuterium
  • Diffraction
  • Diffractometers
  • Hydrogen
  • Military Research
  • Molecular Weight
  • New York
  • Physical Properties
  • Resonance
  • Spectra
  • United States
  • X Rays

Fields of Study

  • Chemistry
  • Materials science

Readers

  • Combustion science or combustion engineering.
  • Molecular and Cellular Biochemistry
  • Semiconductor Device Technology