Non-Destructive Analysis for Hydrogen Concentrations in Materials

Abstract

The objective of the proposed research is to conduct several preliminary experiments to verify calculations made by these investigators that show it to be possible to non-destructively and quantitatively determine hydrogen content in steel and possibly other host materials at the parts per million level (minimum level of from 100 to 1 ppm). The hydrogen analysis is based on the fact that 24 keV neutrons readily penetrate large thicknesses of materials composed mainly of iron with little scattering and the scattering that does occur, is nearly isotropic. However, the presence of a light material (small mass number) such as hydrogen will cause significant scattering of the neutrons in a preferred forward angle, which permits these hydrogen-scattered neutrons to be distinguished from other neutrons by their particular scattering angle and energy. The number of neutrons scattered at angles and energies peculiar to hydrogen will be directly proportional to the concentration of hydrogen in the host material. Thus, the measurement of the number of hydrogen scattered neutrons will permit the quantitative, non-destructive measurement of the hydrogen concentration in test articles or samples and/or whole prototypes.

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Document Details

Document Type
Technical Report
Publication Date
Oct 31, 1991
Accession Number
ADA246098

Entities

People

  • Walter Meyer
  • William H. Miller

Organizations

  • Syracuse University

Tags

Communities of Interest

  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Detection
  • Detectors
  • Engineering
  • Gamma Rays
  • Geometry
  • Hydrogen
  • Materials
  • Measurement
  • Neutron Beams
  • Neutron Spectrum
  • Nuclear Engineering
  • Nuclear Radiation
  • Scattering
  • Spectra
  • Spectrometers
  • Spectroscopy
  • Thickness

Fields of Study

  • Physics

Readers

  • Quantum spin resonance or Electron Paramagnetic Resonance spectroscopy.
  • Radar Systems Engineering.
  • Theoretical Analysis.