Formation, Structure and Properties of Boron Nitride Fibers from Polymer Precursors

Abstract

This report describes a study of possible polymer precursor-based routes to oriented boron nitride fibers, with emphasis on the formation of continuous polyborate gel fibers and subsequent nitridation. Results from preliminary investigations of polyborazylene, polyborazine and decaborane-diamine as precursors for boron nitride fibers are also included. Formation, via a sol-gel route, of a polyborate gel fiber containing no metal counter ion is a major accomplishment of this research. Incorporation in the precursor of rheological aids that are fugitive during subsequent pyrolysis/nitridation is seen to be advantageous in the formation of processable polyborate fibers. Whether suitable schemes exist for generating high orientation in the trial boron nitride fiber remains an unanswered question with all the precursors. Nonoxide precursors suffer, in addition, due to their high cost and chemical instabilities prior to their conversion to BN fibers.

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Document Details

Document Type
Technical Report
Publication Date
Feb 25, 1992
Accession Number
ADA247679

Entities

People

  • A. S. Abhiraman
  • Bruce Wade
  • N. Venkatasubramanian
  • Prashant Desai

Organizations

  • Georgia Tech

Tags

Communities of Interest

  • Advanced Electronics

DTIC Thesaurus Topics

  • Boric Acids
  • Ceramic Materials
  • Chemical Engineering
  • Chemical Reactions
  • Chemical Synthesis
  • Chemistry
  • Electron Microscopy
  • Fiber Spinning
  • Fibers
  • Heat Energy
  • Hydroxides
  • Materials
  • Materials Engineering
  • Materials Laboratories
  • Materials Processing
  • Materials Science
  • Spectroscopy

Fields of Study

  • Materials science

Readers

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