Non-Equilibrium Synthesis by Laser Cladding of Ni, Nb and Mg Alloys for Improved Environmental Resistance

Abstract

The technique of laser surface modification provides a unique means of synthesizing novel nonequilibrium materials in near net shape. The goal of the proposed program is to develop a science base for synthesis of nonequilibrium metastable alloys by laser processing. This report summarizes experimental and theoretical studies carried out during the period of November 1988 to October 1991 on laser surface modification of Ni, Nb and Mg alloys for improved environmental resistance at high temperature. A microstructural evolution model of NbA13 was developed and the relative oxidation resistance of claddings of several Nb-based alloys were investigated. Initial work with V revealed that V increases the ductility, and decreases the oxidation resistance of laser clad NbA13. Oxidation behavior of alloys with Ti, B and Hf as a ternary alloy addition were identified: Oxidation tests at 800, 1200, and 1400 deg C were conducted on NbA13-0 at %B (O B), NbA13-0.5 at %B (0.5 B), NbA13-1.0 at %B (1.0 B), NbA13-1.0 at B-3 at %Ti (3 Ti), NbA13-1.0 at %B-6 at %Ti (6 Ti) and NbA13-1.5 at %Hf (1.5 Hf) alloys. An external layer of (x-alumina formed on samples of alloys 0.5 B and 1.0 B isothermally oxidized in air at 800, 1200 and 1400 deg C. A mixture of alumina and NbA104 formed on the samples of alloy 0 B exposed to same testing conditions.

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Document Details

Document Type
Technical Report
Publication Date
Mar 30, 1992
Accession Number
ADA250552

Entities

People

  • A. Kar
  • C. R. Ribaudo
  • J. Mazumder
  • S. K. Tewari

Organizations

  • University of Illinois Urbana–Champaign

Tags

Communities of Interest

  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Body Weight
  • Chemical Analysis
  • Chemistry
  • Corrosion Resistance
  • Differential Thermal Analysis
  • Diffraction
  • Engineering
  • Materials
  • Materials Engineering
  • Materials Processing
  • Materials Science
  • Mechanical Working
  • Oxidation Resistance
  • Phase Diagrams
  • Phase Transformations
  • Solid Solutions
  • Spectra

Fields of Study

  • Materials science

Readers

  • Fire Suppression Systems Design.
  • Powder metallurgy of Titanium alloys.

Technology Areas

  • Directed Energy
  • Directed Energy - Pulsed-Laser Deposition